Metrohm 732 IC Detector Bedienungsanleitung Seite 127
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4 Operation
732 IC Detector / 733 IC Separation Center
120
• Identification "ZEROREF"
Reference value for the auto-zero function (measured value which is
compensated).
• Identification "OVERLOAD"
The measured value is 50…80% outside the selected full-scale
range.
• Identification "BACKGROUND"
The measured value is more than 80% outside the selected full-scale
range. The absolute conductivity (background) is outputted in place
of the auto-zero value.
Output of individual measured values
• For the output of individual measured values, ">CONFIG/print
meas.value = immed." must be selected (see section 4.4.2). Each
time the <PRINT> key is pressed, a measured value will be out-
putted via the RS232 interface.
• Example:
Individual measured value output with print header output
(with date and time), run time, measured value
>CONFIG/printer
id.1
id.2
print header: always
date&time: on
send to: Seiko
>CONFIG/print meas.value
print crit.: immed.
date&time: off
732 IC Detector 01104 732.0012 Print header
date 1995-10-09 time 13:24:58 Date and time
12.3 138.9 uS/cm Run time, measured value
==============
732 IC Detector 01104 732.0012 Print header
date 1995-10-09 time 13:25:37 Date and time
139.1 uS/cm ZEROREF Auto-zero reference value
13.0 +0.0 uS/cm Run time, auto-zero value
==============
- 732 IC Detector 1
- 733 IC Separation Center 1
- Table of contents 2
- List of figures 6
- 1.2 Parts and controls 10
- 1313121211111010 11
- 1818 1717 1616 1515 1414 11
- IC Separation Center733 12
- FILL INJECT 12
- 1 Introduction 13
- 1.3.1 Organization 15
- >PARAM/detector 16
- 1.4 Safety notes 17
- 2 Installation 18
- 2.2.1 Packaging 19
- 2.2.2 Check 19
- 2.2.3 Location 19
- 6.2125.090 20
- 6.2125.0906.2125.090 22
- 2.4 Mains connection 24
- 2.4.2 Fuses 25
- 2.5 Capillary connections 26
- 50504949 5151 5252 27
- 6.2125.060 28
- 2.6.3 Filter unit PEEK 29
- 2.6.4 Filter unit Manufit 30
- 2222 6464 6565 32
- 6666 65656767 6868 32
- 5656 7070 33
- 2.7 Precolumns 35
- Injektor 36
- 94949090 45
- 1 2 3 4 5 6 7 8 9 50
- 2.9.7 Connection of a PC 51
- 3 Operating tutorial 52
- 3.2 Preparations 53
- 3.3 Putting into operation 55
- ">" and 61
- 151.2 µµS/cm 8.9 min 65
- 151.2 µµS/cm 53.2 min 65
- 3.4 Calibration 66
- OVERLOAD 67
- +0.000 µµS/cm 0.0 min 68
- 3.5 Sample determination 69
- 3.6 Storing as a method 71
- "Water" for 73
- "Water" 73
- 4.2.1 Display 78
- Key field of 732 IC Detector 79
- "active") 80
- "cycle" 80
- ":" 83
- 4.2.3 Instrument dialog 84
- Main menu 84
- Inquiries 84
- 4.2.4 Data entry 86
- 4.2.5 Text entry 87
- ">CONFIG/detector/ 88
- ">CONFIG/ 88
- 4.3.2 Status messages 89
- 4.4 Basic settings 91
- "off °C" 96
- 4.5 Measurement parameters 104
- --------" 105
- "full scale" 106
- "08:34") 107
- 709 = on" 108
- 4.5.2 <FULL SCALE>key 109
- 4.6 Triggering of functions 110
- 4.6.2 <INJECT> keys 111
- ZERO ZERO 112
- ZERO OFF 113
- PUMP R/S 113
- 4.7 Programming 114
- "disabled" 115
- "range", see sec 118
- "full scale", see 118
- TTTTTTTT 119
- "Pmin", see sec 120
- 4.7.2 <PROG R/S> key 121
- 4.7.3 <EVENT> key 121
- "---" means that no 122
- "flag", the program 122
- "prog R/S" 123
- 4.7.4 <METHOD> key 124
- 4.8 Data output 126
- "ZEROREF" 127
- "OVERLOAD" 127
- "BACKGROUND" 127
- ">CONFIG/print 127
- 4.8.2 <PLOT> key 129
- Preparations 129
- Print header 130
- Identification 1 130
- Identification 2 130
- Date and time 130
- 4.8.3 <REPORT> key 131
- 4.9 Examples of methods 133
- General conditions 136
- Configuration 136
- Settings for 709 IC Pump 138
- Settings for 752 Pump Unit 138
- 4 Operation 139
- 5.1.1 Separating columns 140
- 5.1.2 Pumps 141
- 5.1.3 Eluents 142
- 5.1.4 Suppressor module 143
- 5.1.5 Connections 143
- 5.2.1 General information 143
- 5.2.2 Passivation 144
- 5.2.3 Recycling 144
- 5.2.4 Shutdown 144
- 100100999998989797 149
- 5.3 Faults and malfunctions 152
- 5.4 Diagnostic tests 156
- 5.4.2 Prepare instruments 157
- 5.4.4 Check keypad 158
- 5.4.5 Check display 159
- 5.4.6 Check RS232 interfaces 160
- 5.4.8 Internal hardware test 162
- 5.4.9 Initialize data memory 164
- 5.5 Validation / GLP 166
- 6 Interfaces 168
- 6.1.2 Call-up of objects 169
- 6.1.3 Triggers 170
- 6.1.4 Status messages 171
- 6.1.5 Error messages 172
- &Setup.Save" 180
- Check offset $G, $S 182
- >CONFIG/RS 184
- 6.1.8 Handshake 185
- 6.1.9 Pin assignment 188
- HWs". The 189
- 6.3 Analog output 194
- 6.5 Valve interfaces 195
- 7 Appendix 196
- 2.732.0010 200
- 2.732.0110 200
- 16" 201
- 7.3 Optional accessories 203
- 7.4 Warranty and conformity 211
- EU Declaration of Conformity 212
- 7.5 Index 216
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