Metrohm 732 IC Detector Bedienungsanleitung Seite 110
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4.6 Triggering of functions
732 IC Detector / 733 IC Separation Center
103
4.6 Triggering of functions
4.6.1 <FILL> keys
The two <FILL> keys at the 733 IC Separation Center each have the
following function, which depends on the instrument version:
733.0010 (1 valve) 733.0X20 (2 valves) 733.0X30 (valve+ suppr.)
FILL
A
Switching of injection
valve A to "FILL"
position
Switching of injection
valve A to "FILL"
position
Switching of injection
valve A to "FILL"
position
STEP
FILL
B
No function Switching of injection
valve B to "FILL"
position
Switching of suppres-
sor module to next
position ("STEP"
function)
If the injection valve is in the
"FILL" position, the green LED in
the key lights up. In this position
the injection valve is connected
as shown in the diagram oppo-
site:
• The sample loop is filled by
siphoning in the sample so-
lution using the syringe.
• The eluent flows directly to
the separating column.
The "FILL" function can be triggered at any time with the <FILL> key –
also in the edit mode or when a program is running. If this is not re-
quired, the key can be locked. For this, the parameter ">CONFIG/733 IC
Sep.Cent./control" must be set to "732 only" under the <CONFIG>
key (see section 4.4.2). Switching of the injection valve is then possible
only using the 732 IC Detector via a programmed "FILL" command or
with ">CONFIG/733 IC Sep.Cent./trigger = fill".
With the 733.0030 IC Separation Center, switching of the suppressor
module to the next position can be triggered automatically by the
switching of injection valve A to the "FILL" position. For this, the pa-
rameter ">CONFIG/733/suppressor/auto step" must be set to "fill"
under the <CONFIG> key (see section 4.4.2).
12
4 5
3 6
Syringe
Column Eluent
Sample
Loop
- 732 IC Detector 1
- 733 IC Separation Center 1
- Table of contents 2
- List of figures 6
- 1.2 Parts and controls 10
- 1313121211111010 11
- 1818 1717 1616 1515 1414 11
- IC Separation Center733 12
- FILL INJECT 12
- 1 Introduction 13
- 1.3.1 Organization 15
- >PARAM/detector 16
- 1.4 Safety notes 17
- 2 Installation 18
- 2.2.1 Packaging 19
- 2.2.2 Check 19
- 2.2.3 Location 19
- 6.2125.090 20
- 6.2125.0906.2125.090 22
- 2.4 Mains connection 24
- 2.4.2 Fuses 25
- 2.5 Capillary connections 26
- 50504949 5151 5252 27
- 6.2125.060 28
- 2.6.3 Filter unit PEEK 29
- 2.6.4 Filter unit Manufit 30
- 2222 6464 6565 32
- 6666 65656767 6868 32
- 5656 7070 33
- 2.7 Precolumns 35
- Injektor 36
- 94949090 45
- 1 2 3 4 5 6 7 8 9 50
- 2.9.7 Connection of a PC 51
- 3 Operating tutorial 52
- 3.2 Preparations 53
- 3.3 Putting into operation 55
- ">" and 61
- 151.2 µµS/cm 8.9 min 65
- 151.2 µµS/cm 53.2 min 65
- 3.4 Calibration 66
- OVERLOAD 67
- +0.000 µµS/cm 0.0 min 68
- 3.5 Sample determination 69
- 3.6 Storing as a method 71
- "Water" for 73
- "Water" 73
- 4.2.1 Display 78
- Key field of 732 IC Detector 79
- "active") 80
- "cycle" 80
- ":" 83
- 4.2.3 Instrument dialog 84
- Main menu 84
- Inquiries 84
- 4.2.4 Data entry 86
- 4.2.5 Text entry 87
- ">CONFIG/detector/ 88
- ">CONFIG/ 88
- 4.3.2 Status messages 89
- 4.4 Basic settings 91
- "off °C" 96
- 4.5 Measurement parameters 104
- --------" 105
- "full scale" 106
- "08:34") 107
- 709 = on" 108
- 4.5.2 <FULL SCALE>key 109
- 4.6 Triggering of functions 110
- 4.6.2 <INJECT> keys 111
- ZERO ZERO 112
- ZERO OFF 113
- PUMP R/S 113
- 4.7 Programming 114
- "disabled" 115
- "range", see sec 118
- "full scale", see 118
- TTTTTTTT 119
- "Pmin", see sec 120
- 4.7.2 <PROG R/S> key 121
- 4.7.3 <EVENT> key 121
- "---" means that no 122
- "flag", the program 122
- "prog R/S" 123
- 4.7.4 <METHOD> key 124
- 4.8 Data output 126
- "ZEROREF" 127
- "OVERLOAD" 127
- "BACKGROUND" 127
- ">CONFIG/print 127
- 4.8.2 <PLOT> key 129
- Preparations 129
- Print header 130
- Identification 1 130
- Identification 2 130
- Date and time 130
- 4.8.3 <REPORT> key 131
- 4.9 Examples of methods 133
- General conditions 136
- Configuration 136
- Settings for 709 IC Pump 138
- Settings for 752 Pump Unit 138
- 4 Operation 139
- 5.1.1 Separating columns 140
- 5.1.2 Pumps 141
- 5.1.3 Eluents 142
- 5.1.4 Suppressor module 143
- 5.1.5 Connections 143
- 5.2.1 General information 143
- 5.2.2 Passivation 144
- 5.2.3 Recycling 144
- 5.2.4 Shutdown 144
- 100100999998989797 149
- 5.3 Faults and malfunctions 152
- 5.4 Diagnostic tests 156
- 5.4.2 Prepare instruments 157
- 5.4.4 Check keypad 158
- 5.4.5 Check display 159
- 5.4.6 Check RS232 interfaces 160
- 5.4.8 Internal hardware test 162
- 5.4.9 Initialize data memory 164
- 5.5 Validation / GLP 166
- 6 Interfaces 168
- 6.1.2 Call-up of objects 169
- 6.1.3 Triggers 170
- 6.1.4 Status messages 171
- 6.1.5 Error messages 172
- &Setup.Save" 180
- Check offset $G, $S 182
- >CONFIG/RS 184
- 6.1.8 Handshake 185
- 6.1.9 Pin assignment 188
- HWs". The 189
- 6.3 Analog output 194
- 6.5 Valve interfaces 195
- 7 Appendix 196
- 2.732.0010 200
- 2.732.0110 200
- 16" 201
- 7.3 Optional accessories 203
- 7.4 Warranty and conformity 211
- EU Declaration of Conformity 212
- 7.5 Index 216
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