Metrohm 850 Professional IC Anion MSM-HC Bedienungsanleitung

850 Professional ICAnion – MSM-HC 2.850.2050Manual8.850.8016EN

Table of figures￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VIII￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCFigure 46 Pump tubing connection – Changing the filter ...

5.11 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭90￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC123 45Figure 45 MSM-HC – Compon

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭91￭ Check whether solution emerges at the MSM-HC connecting

5.11 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭92￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC5.11.3.3 Replacing parts of th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭93￭ Insert the new MSM-HC rotor A (45-3) in the MSM-HC hous

5.12 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭94￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCCautionThe 6.1826.xxx pump tubings consist of PVC or PP and the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭95OrdernumberName Material InnerdiameterUse6.1826.330 Pump

5.13 Conductivity detector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭96￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC 3Mounting filter screw￭ Screw the filter screw (46-3) bac

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭97special IC applications in the corresponding "Applic

5.15 Quality Management and validation with Metrohm￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭98￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC5.15 Quality Management and vali

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭996 Troubleshooting6.1 Problems and their solutionsProblem Cause Re

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe instrument 850 Profession

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭100￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCProblem Cause RemedyEluent – Evaporation of theorga

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭101Problem Cause RemedyMSM-HC – regeneration orrinsing solution flow

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭102￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCProblem Cause RemedyExtreme spread ofthe peaks in t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭103Problem Cause Remedy￭ Connect an FEP tubing between the ICinstrume

7.1 Reference conditions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭104￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC7 Technical specifications7.1 Reference conditionsThe tec

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭1057.5 HousingDimensionsWidth 365 mmHeight 642 mmDepth 380

7.8 Sample degasser￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭106￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCPressure rangePump 0…50.0 MPa (0…500 bar)Pump head 0…35.0 MPa (0

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭1077.10 Column thermostatType Peltier technique thermostat

7.13 Conductivity measuring system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭108￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC7.13 Conductivity measuring systemType ￭ Micropr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭1097.14 Mains connectionRequired voltage 100…240 V ± 10 % (

1.1 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCused for the purpose of protecting other sensitive componen

7.16 Safety specification￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭110￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC7.16 Safety specificationDesign / Test ￭ EN/IEC/UL 61010-

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭1118 Conformity and warranty8.1 Declaration of ConformityTh

8.2 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭112￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCEN 61010-1 Safety requirements for electrical equi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭113Software developmentSoftware development occurs in terms o

8.3 Warranty (guarantee)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭114￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCFaults arising from circumstances that are not the responsi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭1159 AccessoriesCautionSubject to change without notice!9.1 Scope of de

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭116￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCQty. Order no. Description2 6.1608.020 Glass bottle / 1000 mL

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭117Qty. Order no. Description1 6.1803.040 PTFE capillary 0.5 mm i.d. / 1

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭118￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCQty. Order no. Description2 6.1816.020 Silicone tubing 6 mm i.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭119Qty. Order no. Description1 6.2617.010 Tool for piston sealFor removin

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭31.2 Intended useThe 850 Professional IC Anion – MSM-HC is used for the

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭120￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCQty. Order no. Description1 6.2621.080 Capillary cutterFor pla

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭121Qty. Order no. Description1 6.2743.080 Stopper for overflow (ProfIC),

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭122￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCQty. Order no. Description1 6.2744.040 2 x UNF 10/32 couplingF

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭123Qty. Order no. Description1 6.2744.210 Tubing adaptor for aspiration f

9.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭124￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCQty. Order no. Description1 8.850.8016EN Manual for 850 Pro

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭125Order no. Descriptionregulation 21 CFR part 11 as well as GLP. Dialog

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭126￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCIndexNumbers/Symbols6.2821.090 aspiration filter ... 726.2821.130 filter ..

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭127IIC columnsee also "Separation column"...

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭128￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCSample degasserInstallation ... 44Operation ...

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCWarningThis symbol draws attention to a possible hazard dueto

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭5WarningNever open the housing of the instrument. The instrument could b

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC1.4.4 Flammable solvents and chemicalsWarningAll relevant saf

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭72 Overview of the instrument2.1 Front9123546781011Figur

2.1 Front￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3Purge valveFor deaerating the high pressure pump (seeChapter 3.10.1, page 3

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭92.2 Rear12221219201017157654318119121381416Figure 2 Rear

2.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3Mains switchFor switching the instrument on and off.I = ON0 = OFF4Mains con

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭11CautionWhen connecting an instrument to the MSB connecto

3.1 About this chapter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3 Installation3.1 About this chapterThe Installation chapter

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭13 3Connecting the eluent path￭ Equip the 6.1834.080 eluent aspiration t

3.2 Initial installation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC￭ Connect the 6.1803.020 aspirating capillary for rinsing so

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭15￭ Connect guard column (optional) (see Chapter 3.20, page 62)– Fasten

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC122234567891011121314151617181818181819202122Figure 3 Instal

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭173MSM-HC eluent inlet capillaryLabeled with Eluent.4MSM-HC eluent outle

3.5 Capillary connections in the IC system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3.4.3 LocationThe instrument has been dev

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭19NoteFor an improved overview, capillary and tubing connections can beb

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Professional ICAnion – MSM-HC 2.850.2

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3.6 Rear of the instrument3.6.1 Rollers and handleIn ord

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭21Removing rollersProceed as follows to remove the rollers: 1Remove knur

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC211Figure 6 Handle as MPak holder1Knurled screwsFor fasten

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭233.6.2 Positioning and connecting the detectorDetector 1Detector 24444

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCNoteUp to two detectors can be positioned and connected.Ca

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭25￭ Connect the detector cable to the detector connection socketDetector

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC123Figure 8 Connection for the leak sensor on the rear of

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭27245613798Figure 9 Drainage tubing1Drainage tubing connectionFor draini

3.7 Capillary and cable feed-throughs￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC7Drainage tubingSection of the 6.1816.020 silic

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭29212134Figure 10 Capillary feed-throughs on the doors1Luer connectorsFo

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.7 Capillary and cable feed-throughs￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC1234567 88 76 59101112 1211109FrontRearFigure 1

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭313.8 Eluent3.8.1 Connecting eluent bottleThe eluent is aspirated out

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC1 234Figure 12 Installing eluent bottle attachment1Eluent aspiration tubin

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭33 4Installing tubing weighting and aspiration filter1 2345Figure 14 Ins

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC￭ Fasten the bottle attachment (14-2) on the eluent bottle (16-10).The asp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭355Eluent6Aspiration filter 6.2821.0907Filter holderFrom accessory set 6

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3Tubing flareWith tubing nipple.4Clamping screw5Eluent aspira

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭3710891234562722211212213Figure 18 Capillary connections high pressure p

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCNoteThe eluent aspiration tubing is already installed in the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭393.10.2 Deaerating the high pressure pumpThe high pressure pump will o

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument description ...

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCDeaerating the high pressure pumpThe instrument must be conne

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭41 4Setting the flow rate￭ Start MagIC Net (if not yet started).￭ Ensure

3.12 Pulsation damper￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCInstalling the inline filterCautionObserve the flow direction m

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭43The pulsation damper protects the separation column from damagecaused

3.13 Sample degasser￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3.13 Sample degasserThe sample degasser removes gas bubbles and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭45 4Guide the other end of the connection capillary out of the instrumen

3.14 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3Connection capillaryConnected to connector 4. Carries eluent to

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭47124 53 6124 53 6124354312A BFigure 25 Injection valve – PositionsAPosi

3.15 Column thermostat￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3.15 Column thermostatThe column thermostat controls the temp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭4913211112Figure 26 Column thermostat1Capillary feed-throughsFor guiding

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3.11 Inline filter ...

3.15 Column thermostat￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCNoteThe column input capillary is already threaded into the ca

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭513.16 High Capacity Metrohm Suppressor Module(MSM-HC)3.16.1 General i

3.16 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC13234567821Figure 27 MSM-HC – C

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭53Connecting the capillaries of the MSM-HC 1Connecting the eluent inlet

3.17 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3.17 Peristaltic pump3.17.1 Principle of the peristaltic pump

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭553.17.2 Installing the peristaltic pump6.2744.16016.2744.1802 3 4 5 6

3.17 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC 3Connecting the pressure sideNoteDepending on the use of the p

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭57123Figure 31 Install pump tubing connection without filter1Union nut2A

3.17 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCPump tubing Adapter6.1826.340 (black/black)6.1826.360 (white/wh

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭593.18 Conductivity detectorThe conductivity detector continuously meas

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭V5.6 Inline filter ...

3.18 Conductivity detector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC132Figure 33 Conductivity detector rear1Detector cableWith

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭611 234Figure 34 Connection Detector – MSM-HC1Detector inlet capillary2M

3.20 Guard column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC1Connecting the mains cable￭ Plug the mains cable into the mains co

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭63NoteThe guard column may only be installed after the initial start-up

3.21 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC3.21 Separation columnThe intelligent separation column (iCol

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭65Connecting and rinsing the separation column 1Connecting the separatio

4.1 Initial start-up￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC4 Start-upThe chapter Start-up is divided into 2 sections:Initi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Start-up850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭67 4Setting the contact pressure of the peristaltic pumpNoteThis work step n

4.2 Conditioning￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC 2Preparing the instrument￭ Ensure that the column is correctly moun

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭695 Operation and maintenance5.1 General information5.1.1

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC7.11 High Capacity Metrohm Suppressor Module(MSM-HC) ...

5.2 Capillary connections￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC5.1.3 OperationCautionIn order to avoid disturbing tempera

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭715.3 DoorCautionThe door is made of PMMA (polymethylmetac

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC5.4.2 Operation5.4.2.1 Supply bottleThe supply bottle with t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭73CautionIn order to spare the pump seals, the pump should

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCCleaning/replacing the zirconium oxide pistonClean one piston

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭75￭ Remove the backup ring from the pump head and lay to th

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCparts: a tip for removing the old piston seal and a sleeve for

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭7712Figure 38 Removing the piston seal1Piston seal2Tool for

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭78￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC12Figure 40 Inserting the piston seal into the pump head 4Repl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭791234Figure 41 Removing valves1Outlet valve holder2Outlet

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭VIITable of figuresFigure 1 Front 850 Professional IC – Anion – MSM-HC

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭80￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC￭ Place the valve with the seal faced downwards above the rece

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭81123567891098710546Figure 43 Components of the inlet valve

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭82￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC￭ Place the valve housing over the stacked components and hold

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭83Mounting the pump headNoteTo prevent the pump head from b

5.6 Inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭84￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCChanging the filterThe flow must be stopped before changing the fil

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭855.7 Inline sample preparationTo protect the separation c

5.8 Rinsing the sample path￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭86￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC 2Aspirating the sample and measuring timeAspirate a samp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭875.9 Sample degasser5.9.1 OperationIf you are working wi

5.11 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭88￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HCThe MSM-HC consists of 3 suppre

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC￭￭￭￭￭￭￭￭89 2Regenerating the MSM-HCCautionThe pump tubings made of