Metrohm 861 Advanced Compact IC Bedienungsanleitung

861 Advanced Compact IC Instructions for Use8.861.1033 CH-9101 Herisau/Switzerland E-Mail [email protected] Internet www.metrohm.com

Table of contents 861 Advanced Compact IC / Instructions for Use 8.861.1033 VI 69 CO2 absorber 70 Cotton wool 71 SGJ clip 72 Absorber tube 73

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 90 5.1.15 Housing Material of cover Polyurethane rigid foam (PUR) with fir

5.2 Standard equipment 861 Advanced Compact IC / Instructions for Use 8.861.1033 915.2 Standard equipment Subject to changes ! All dimensions are

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 92 Number Order no. Description 2.861.0010 2.861.0020 2.861.0040 1

5.2 Standard equipment 861 Advanced Compact IC / Instructions for Use 8.861.1033 93Number Order no. Description 2.861.0010 2.861.0020 2.861.00

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 94 Number Order no. Description 2.861.0010 2.861.0020 2.861.0040 - -

5.2 Standard equipment 861 Advanced Compact IC / Instructions for Use 8.861.1033 95Number Order no. Description 2.861.0010 2.861.0020 2.861.00

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 96 Number Order no. Description 2.861.0010 2.861.0020 2.861.0040 1

5.3 Optional accessories 861 Advanced Compact IC / Instructions for Use 8.861.1033 97Order no. Description 6.2744.040 PEEK coupling For connect

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 98 Order no. Description 6.2824.070 Zircon piston Spare part for 6.2824.

5.3 Optional accessories 861 Advanced Compact IC / Instructions for Use 8.861.1033 99Order no. Description 6.1006.120 Metrosep Anion Dual 3 An

1.1 Instrument description 861 Advanced Compact IC / Instructions for Use 8.861.1033 1 1 Introduction 1.1 Instrument description The 861 Advanc

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 100 Order no. Description 6.1010.240 Metrosep C2 S-Guard Separate guard

5.3 Optional accessories 861 Advanced Compact IC / Instructions for Use 8.861.1033 101Number Order No. Description 1 6.2744.070 PEEK compress

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 102 5.4 Warranty and Conformity 5.4.1 Warranty The warranty on our produc

5.4 Warranty and Conformity 861 Advanced Compact IC / Instructions for Use 8.861.1033 1035.4.2 Declaration of Conformity This is to certify the

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 104 5.4.3 Quality Management Principles Metrohm Ltd., CH-9101 Herisau, S

5.5 Index 861 Advanced Compact IC / Instructions for Use 8.861.1033 1055.5 Index <Inject>... 54 6.2621

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 106 Connection diagram ...14 Connection for detector blo

5.5 Index 861 Advanced Compact IC / Instructions for Use 8.861.1033 107Inlet valve 99 Cleaning ... 74 Figure...

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 108 Program steps ...58 Protection class ...

5.5 Index 861 Advanced Compact IC / Instructions for Use 8.861.1033 109Mounting... 80 Suppressor inlet capillary

1 Introduction 861 Advanced Compact IC / Instructions for Use 8.861.1033 2 All components which come into contact with eluent and sample are met

1.2 Parts and controls 861 Advanced Compact IC / Instructions for Use 8.861.1033 3 1.2 Parts and controls In this Section you will find the numb

1 Introduction 861 Advanced Compact IC / Instructions for Use 8.861.1033 4 1.2.2 Rear panel Figure 2: Rear panel 861 Advanced Compact IC7Openin

1.2 Parts and controls 861 Advanced Compact IC / Instructions for Use 8.861.1033 5 21Remote interface Remote-I/O lines for connection of ex-tern

1 Introduction 861 Advanced Compact IC / Instructions for Use 8.861.1033 6 1 Door to inner compartment 24Inlet capillary for injection valve PEE

1.2 Parts and controls 861 Advanced Compact IC / Instructions for Use 8.861.1033 7 1.2.4 Interior 2.861.0020 Figure 4: Interior of the IC 2.861

1 Introduction 861 Advanced Compact IC / Instructions for Use 8.861.1033 8 27 Sample loop 20 µL PEEK sample loop 6.1825.210 28 Injection valve

1.2 Parts and controls 861 Advanced Compact IC / Instructions for Use 8.861.1033 9 1.2.5 Interior 2.861.0040 Figure 5: Interior of the IC 2.861.

1 Introduction 861 Advanced Compact IC / Instructions for Use 8.861.1033 10 27 Sample loop 20 µL PEEK sample loop 6.1825.210 28 Injection valve

1.3 Information on the Instructions for Use 861 Advanced Compact IC / Instructions for Use 8.861.1033 111.3 Information on the Instructions for U

1 Introduction 861 Advanced Compact IC / Instructions for Use 8.861.1033 12 1.3.2 Notation and pictograms The following notations and pictograms

1.4 Safety notes 861 Advanced Compact IC / Instructions for Use 8.861.1033 131.4 Safety notes 1.4.1 Electrical safety While electrical safety in

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 14 2 Installation 2.1 Overview 2.1.1 Flow chart The following flow char

2.1 Overview 861 Advanced Compact IC / Instructions for Use 8.861.1033 15Figure 6: Connecting diagram for 2.861.0010 Compact IC without suppres-

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 16 Figure 8: Connecting diagram for 2.861.0040 Compact IC with suppre

2.3 Attaching the accessories 861 Advanced Compact IC / Instructions for Use 8.861.1033 17 To avoid disturbing temperature influences on the insu

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 18 2.3.2 Connection of syringe and aspirating tubing For manual fillin

2.3 Attaching the accessories 861 Advanced Compact IC / Instructions for Use 8.861.1033 19These PEEK connectors can also be used to connect 6.1822

CH-9101 Herisau/Switzerland E-Mail [email protected] Internet www.metrohm.com 861 Advanced Compact IC 8.861.1033 Instructions for Use

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 20 Figure 10: 6.2821.120 Filter unit PEEK 34 Filter unit PEEK (6.2821

2.4 Mains connection 861 Advanced Compact IC / Instructions for Use 8.861.1033 212.4 Mains connection Follow the instructions below for connecti

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 22 Figure 11: Setting the mains voltage 2.4.2 Fuses One of the two fu

2.5 Connection to PC 861 Advanced Compact IC / Instructions for Use 8.861.1033 232.5 Connection to PC 2.5.1 Connecting cable Always switch off 8

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 24 2.5.3 First Login Starting and closing of the Software is described

2.6 High-pressure pump 861 Advanced Compact IC / Instructions for Use 8.861.1033 252.6 High-pressure pump In order to avoid damage to the pump it

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 26 Figure 12: Connection of the pulsation dampener 24 Inlet capillary

2.6 High-pressure pump 861 Advanced Compact IC / Instructions for Use 8.861.1033 27tory filled with either isopropanol or methanol/water). If this

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 28 861 Advanced Compact IC, cut off to the required length and push at

2.6 High-pressure pump 861 Advanced Compact IC / Instructions for Use 8.861.1033 29 • Select the Connect to workplace item of the Control menu in

Teachware Metrohm AG Oberdorfstrasse 68 CH-9101 Herisau [email protected] 1. Edition 2005 These instructions are protected by copyright. All r

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 30 sure pump. • Close the rotary knob on purge valve 37 by turning it

2.7 Precolumns and separating columns 861 Advanced Compact IC / Instructions for Use 8.861.1033 311 Connect precolumn • Remove end caps from th

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 32 Anion columns 100 µL Cation columns 10 µL Columns for suppressor

2.7 Precolumns and separating columns 861 Advanced Compact IC / Instructions for Use 8.861.1033 33 Figure 14: Installation of column without supp

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 34 3 Connect column to suppressor module «MSM II» • Screw the outle

2.8 Suppressor module «MSM II» 861 Advanced Compact IC / Instructions for Use 8.861.1033 352.8.2 Preparation of the peristaltic pump Before start

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 36 Figure 15: Installing pump tubings 47 Tubing cartridge (6.2755.00

2.8 Suppressor module «MSM II» 861 Advanced Compact IC / Instructions for Use 8.861.1033 37Figure 16: Connection of separation column with suppre

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 38 50 Snap-action lever for releasing the tubing cartridge 51 Pump driv

2.8 Suppressor module «MSM II» 861 Advanced Compact IC / Instructions for Use 8.861.1033 392) from above and pull it sufficiently far into the int

Table of contents 861 Advanced Compact IC / Instructions for Use 8.861.1033 I Table of contents 1 Introduction ...

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 40 Figure 17: Connection of supply bottles 2.8.4 Connection of the s

2.8 Suppressor module «MSM II» 861 Advanced Compact IC / Instructions for Use 8.861.1033 41module «MSM II» 46 from below through one of the openin

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 42 2.9 853 CO2 Suppressor More detailed information about the 853 CO2

2.10 Putting into operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 431 Electrical connection 853 – 861 • Use the 6.2143.2

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 44 • Select the Connect to workplace item from the Control menu of th

2.10 Putting into operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 453 Start system • Make sure, that the aspirating tubing

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 46 • Select Connect to workplace in the Control menu in this window.2

2.10 Putting into operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 47Section 3.3.1), the 853 will start up. At the same time a

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 48 2.11 Connection of external devices 2.11.1 Connection of the 838 A

2.11 Connection of external devices 861 Advanced Compact IC / Instructions for Use 8.861.1033 49• Add the 838 Advanced Sample Processor to the sy

Table of contents 861 Advanced Compact IC / Instructions for Use 8.861.1033 II 2.8 Suppressor module «MSM II» ...

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 50 double-click on the 838 icon or via the right-hand mouse key open).

2.11 Connection of external devices 861 Advanced Compact IC / Instructions for Use 8.861.1033 51 On Version 2.861.0040 the 853 CO2 Suppressor is a

2 Installation 861 Advanced Compact IC / Instructions for Use 8.861.1033 52 selected at the 813 (see 813 Instructions for Use, Section 3.4). The

3.1 «IC Net» - Terms 861 Advanced Compact IC / Instructions for Use 8.861.1033 533 Operation This Section describes only the most important poin

3 Operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 54 3.2.2 Connect a system The selected system must be linked to the wor

3.2 Measuring operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 55Open Opens the window for System Settings. Hardware Opens

3 Operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 56 3.3 Settings 3.3.1 Instrument control for connected system A double-cl

3.3 Settings 861 Advanced Compact IC / Instructions for Use 8.861.1033 57Suppressor Suppressor module «MSM II» (inactive with version 2.861.0010

3 Operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 58 Time program On the Program tab of the system settings window a user-de

3.3 Settings 861 Advanced Compact IC / Instructions for Use 8.861.1033 59List of program instructions The following program instructions can be a

Table of contents 861 Advanced Compact IC / Instructions for Use 8.861.1033 III5.1.1 Conductivity measurement ...

3 Operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 60 Remote configuration On the Remote configuration subtab user-defined re

3.3 Settings 861 Advanced Compact IC / Instructions for Use 8.861.1033 61Configuration The Configuration tab in the system settings window contai

3 Operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 62 Links The Links tab in the window for the system settings serves to se

3.3 Settings 861 Advanced Compact IC / Instructions for Use 8.861.1033 63Thermostat Operating temperature of the conductivity cell. Selection: 2

3 Operation 861 Advanced Compact IC / Instructions for Use 8.861.1033 64 Outputs The Outputs tab of the hardware settings window defines remote

3.3 Settings 861 Advanced Compact IC / Instructions for Use 8.861.1033 65Alarm stops The Alarm stops tab of the hardware settings window defines

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 66 4 Notes - Maintenance - Faults 4.1 Practical notes

4.1 Practical notes on ion chromatography 861 Advanced Compact IC / Instructions for Use 8.861.1033 67Storage Always store the separating columns

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 68 low buffering capacity one should preferably use a C

4.2 Maintenance and servicing 861 Advanced Compact IC / Instructions for Use 8.861.1033 69Operation The suppressor module «MSM II» comprises a tot

Table of contents 861 Advanced Compact IC / Instructions for Use 8.861.1033 IV List of figures Figure 1: Front 861 Advanced Compact IC...

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 70 Although constructional measures have been designed

4.2 Maintenance and servicing 861 Advanced Compact IC / Instructions for Use 8.861.1033 71rinsed free from salt with methanol/water (1:4) to avoid

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 72 • Unscrew column 73 from column connection capillar

4.2 Maintenance and servicing 861 Advanced Compact IC / Instructions for Use 8.861.1033 73 To prevent the piston 91 suddenly jumping out of the p

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 74 Figure 20: Replacement of the piston seal 98 40 Pu

4.2 Maintenance and servicing 861 Advanced Compact IC / Instructions for Use 8.861.1033 75the upper opening in the valve housing. The individual c

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 76 Figure 21: Components of inlet valve 99 and outle

4.2 Maintenance and servicing 861 Advanced Compact IC / Instructions for Use 8.861.1033 77 0.1 mol/L H2SO4 / 0.1 mol/L oxalic acid / acetone 5%

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 78 the connection piece 112 (order number 6.2832.010).

4.2 Maintenance and servicing 861 Advanced Compact IC / Instructions for Use 8.861.1033 79111Screw nut 112Connection piece (6.2832.010) with input

Table of contents 861 Advanced Compact IC / Instructions for Use 8.861.1033 V List of numbered parts and controls 1 Door to interior 2 Connecti

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 80 one of the openings of the holder. • If the rotor h

4.2 Maintenance and servicing 861 Advanced Compact IC / Instructions for Use 8.861.1033 81• Insert the new pump tubing 78 or 79 in the tubing car

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 82 4.3 Faults and malfunctions 4.3.1 Error messages If

4.3 Faults and malfunctions 861 Advanced Compact IC / Instructions for Use 8.861.1033 83Malfunction Cause Rectification Extreme peak broadening,

4 Notes - Maintenance - Faults 861 Advanced Compact IC / Instructions for Use 8.861.1033 84 4.4 Diagnostic tests / Validation / GLP The require

5.1 Technical data 861 Advanced Compact IC / Instructions for Use 8.861.1033 855 Appendix 5.1 Technical data Unless otherwise specified, the pub

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 86 Max. temperature deviation ± 2.5°C Heating time ≥ 30 min Temperature s

5.1 Technical data 861 Advanced Compact IC / Instructions for Use 8.861.1033 87Minimum pressure limit adjustable between 0.1 ... 35.0 MPa (1...3

5 Appendix 861 Advanced Compact IC / Instructions for Use 8.861.1033 88 Pin assignment 5.1.9 Analog output Connector Dsub 9 pin (female) 5 196

5.1 Technical data 861 Advanced Compact IC / Instructions for Use 8.861.1033 89Potentials 5.1.11 Mains connection Voltage 115 V: 100...120 V ±