Metrohm 850 Professional IC MSM-HC MCS Prep 3 Bedienungsanleitung

850 Professional ICAnion – MSM-HC – MCS – Prep 3 – 2.850.2180Manual8.850.8025EN

Table of figures￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VIII￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Figure 45 Tool for piston seal 6.2617.010 ...

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭90￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3￭ Place the valve with the seal faced downwards

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭91123567891098710546Figure 51 Components of

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭92￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3￭ Place the valve housing over the stacked comp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭93Mounting the pump headNoteTo prevent the p

5.6 Inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭94￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Changing the filterThe flow must be stopped before c

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭955.7 Inline sample preparationTo protect t

5.8 Rinsing the sample path￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭96￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 2Aspirating the sample and measuring time

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭975.9 Sample degasser5.9.1 OperationIf you

5.10 Sample preparation module (SPM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭98￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3CautionIn the case of reduced cap

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭99 3Connecting the SPM to the IC system￭ Rec

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭11 Introduction1.1 Instrument descriptionThe instrument

5.10 Sample preparation module (SPM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭100￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3￭ Pull the SPM connecting piece

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭101 7Inserting the SPM connecting piece￭ Ins

5.10 Sample preparation module (SPM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭102￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 4Inserting the new SPM rotor AC

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1035.11 Peristaltic pump5.11.1 OperationTh

5.11 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭104￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Table 2 Pump tubingOrdernumberName Material Inn

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭105123Figure 54 Pump tubing connection – Cha

5.13 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭106￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 35.13 High Capa

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1075.13.3 Maintenance5.13.3.1 Regenerating

5.13 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭108￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 3Connecting th

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭109￭ Pull the MSM-HC connecting piece (55-2)

1.1 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Inline filterInline filters protect the sepa

5.13 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭110￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 7Inserting the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭111 3Cleaning the new MSM-HC rotor A￭ Clean

5.14 Metrohm CO2 suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭112￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 35.14 Metrohm CO2 suppressor (MCS)5

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1135.15 Conductivity detector5.15.1 Mainte

5.16 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭114￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 35.16.2 ProtectionTo protect the separation co

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1155.17 Quality Management and validation w

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭116￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 36 Troubleshooting6.1 Problems and

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭117Problem Cause RemedyEluent – Evaporation of theorga

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭118￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Problem Cause RemedyMCS – vacuum pum

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Troubleshooting850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭119Problem Cause Remedy￭ Replace separation column (se

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭3Conductivity detectorThe conductivity detector continuou

6.1 Problems and their solutions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭120￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Problem Cause RemedyUnexpected chang

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1217 Technical specifications7.1 Reference

7.5 Housing￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭122￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 37.5 HousingDimensionsWidth 365 mmHeight 642 mmDepth 380

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭123Pressure rangePump 0…50.0 MPa (0…500 bar)P

7.10 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭124￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 37.10 Peristaltic pumpType 2-channel peristalti

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1257.13 High Capacity Metrohm Suppressor Mod

7.16 Mains connection￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭126￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3ConductivitydetectorCell volume 0.8 µLCell cons

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1277.17 InterfacesUSBInput 1 USB upstream, t

7.20 Weight￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭128￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3￭ EN/IEC 61000-4-11￭ EN/IEC 61000-4-14￭ NAMUR: 20067.20

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1298 Conformity and warranty8.1 Declaration

1.3 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 31.3 About the documentationCautionPlease r

8.2 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭130￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3EN 61010-1 Safety requirements for

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭131Software developmentSoftware development oc

8.3 Warranty (guarantee)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭132￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Faults arising from circumstances that are n

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1339 AccessoriesCautionSubject to change without notice!9

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭134￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Qty. Order no. Description4 6.1608.020 Glass bo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭135Qty. Order no. Description1 6.1803.040 PTFE capillary 0

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭136￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Qty. Order no. Description2 6.1816.020 Silicone

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭137Qty. Order no. Description1 6.2057.080 Adsorption cartr

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭138￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Qty. Order no. Description1 6.2621.030 Hexagon

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭139Qty. Order no. Description1 6.2626.000 Drain nozzle (Pr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭51.4 Safety instructions1.4.1 General notes on safetyWa

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭140￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Qty. Order no. Description1 6.2744.020 Luer/UNF

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭141Qty. Order no. Description3 6.2744.070 Pressure screw s

9.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭142￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Qty. Order no. Description1 6.2816.020 Syringe

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭143Qty. Order no. Description1 6.2837.000 CO2 adsorber car

9.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭144￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 39.2 Optional accessories 2.850.2180 850 Pr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭145Order no. DescriptionFrench, Chinese, Korean, Japanese

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭146￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3IndexNumbers/Symbols6.2821.090 aspiration filter ... 826.282

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭147Technical specifications ... 122Tubing connection ...

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭148￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3QQuality Management ... 115RReference conditions ...

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Protection against electrostatic chargesWarning

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭7More details about the disposal of your old equipment ca

2.1 Front￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 32 Overview of the instrument2.1 Front912354678101112131415F

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭93Purge valveFor deaerating the high pressu

2.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 32.2 Rear12221219201017157654318119121381416Figure 2 Rear 850

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭113Mains switchFor switching the instrument

2.2 Rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3CautionWhen connecting an instrument to the MSB connector (2-

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭133 Installation3.1 About this chapterThe Installation

3.2 Initial installation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3￭ Connect drainage tubings (see Chapter 3.6.5

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭15 6Connecting the instrument￭ Connect the instrument to

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.3 Installation diagramThe following instal

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭171222458910121415161718193333111362122720232427283112529

3.3 Installation diagram￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33PEEK pressure screw, short 6.2744.0704MSM-HC

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭1931SPM sample aspirating capillaryConnect it to the samp

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Professional ICAnion – MSM-HC – MCS –

3.5 Capillary connections in the IC system￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3412 3Figure 4 Connection of

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭21CautionFor the capillary connections between the inject

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3321145Figure 5 Rollers and handle1Knurled s

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭23Mounting handle as MPak holderNoteWhen extended, the ha

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.6.2 Positioning and connecting the detec

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭25NoteUp to two detectors can be positioned and connected

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3￭ Connect the detector cable to the detecto

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭27123Figure 8 Connection for the leak sensor on the rear

3.6 Rear of the instrument￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3245613798Figure 9 Drainage tubing1Drainage

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭297Drainage tubingSection of the 6.1816.020 silicon tubin

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.7 Capillary and cable feed-throughs￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3212134Figure 10 Capillary feed-t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭311234567 88 76 59101112 1211109FrontRearFigure 11 Capill

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.8 Eluent3.8.1 Connecting eluent bottleThe eluent is asp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭331 234Figure 12 Installing eluent bottle attachment1Elue

3.8 Eluent￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 4Installing tubing weighting and aspiration filter1 2345Fi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭35￭ Fasten the bottle attachment (14-2) on the eluent bot

3.9 Eluent degasser￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 35Eluent6Aspiration filter 6.2821.0907Filter holder

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭373Tubing flareWith tubing nipple.4Clamping screw5Eluent

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 310891234562722211212213Figure 18 Capillary con

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭39NoteThe eluent aspiration tubing is already installed i

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument d

3.10 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.10.2 Deaerating the high pressure pumpThe h

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭41Deaerating the high pressure pumpThe instrument must be

3.11 Inline filter￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 4Setting the flow rate￭ Start MagIC Net (if not ye

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭43Installing the inline filterCautionObserve the flow dir

3.12 Pulsation damper￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3The pulsation damper protects the separation col

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭453.13 Sample degasserThe sample degasser removes gas bu

3.14 Sample preparation module (SPM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 4Guide the other end of the conn

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭4713234567821Figure 24 SPM – Connectors1Union nut2SPM con

3.14 Sample preparation module (SPM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.14.3 Inline sample preparation

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭491ABDCFigure 25 Cation exchange with the SPM1SampleASPMB

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.11 Inline filter ...

3.14 Sample preparation module (SPM)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Weak alkaline solutions can direc

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭51￭ The analyte ions are retained on the preconcentration

3.15 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3DPreconcentration columnESeparation columnFMSM-H

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭535Tubing cartridges 6.2755.0006Contact pressure lever7Sn

3.15 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 3Connecting the pressure sideNoteDepending on t

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭55123Figure 33 Install pump tubing connection without fil

3.15 Peristaltic pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Pump tubing Adapter6.1826.340 (black/black)6.182

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭573.16 Injection valveThe injection valve connects the e

3.16 Injection valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Replacing the sample loopThe sample loop can be r

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭591Eluent inputCapillary coming from the high pressurepum

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭V5.3 Door ...

3.17 Column thermostat￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 313211112Figure 36 Column thermostat1Capillary f

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭61NoteThe column input capillary is already threaded into

3.18 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.18 High Capac

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭6313234567821Figure 37 MSM-HC – Connectors1Union nut2MSM-

3.18 High Capacity Metrohm Suppressor Module (MSM-HC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Connecting the c

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭653.19 Metrohm CO2 suppressor (MCS)3.19.1 General infor

3.19 Metrohm CO2 suppressor (MCS)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33Aspirating capillaryFor aspirating

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭67938 7312 33456Figure 39 Adsorption cartridge holder1PEE

3.20 Conductivity detector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 2Removing the caps￭ Remove the two locking

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭69213Figure 40 Conductivity detector front1IC detector 1.

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 37 Technical specifications 1217.1 Reference condit

3.20 Conductivity detector￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3132Figure 41 Conductivity detector rear1Det

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭713 21Figure 42 Connection detector – MCS1Detector input

3.22 Guard column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3The mains cable is three-core and provided with a pl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭73NoteThe guard column may only be installed after the in

3.23 Separation column￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 33.23 Separation columnThe intelligent separati

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭75Connecting and rinsing the separation column 1Connectin

4.1 Initial start-up￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 34 Start-upThe chapter Start-up is divided into 2

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Start-up850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭77 4Setting the contact pressure of the peristaltic pumpNoteT

4.2 Conditioning￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭78￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3 2Preparing the instrument￭ Ensure that the column is

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭795 Operation and maintenance5.1 General i

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭VIITable of figuresFigure 1 Front 850 Professional IC –

5.2 Capillary connections￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭80￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 35.1.3 OperationCautionIn order to avoid dis

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭815.3 DoorCautionThe door is made of PMMA (

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭82￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 35.4.2 Operation5.4.2.1 Supply bottleThe suppl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭83CautionIn order to spare the pump seals, t

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭84￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3Cleaning/replacing the zirconium oxide pistonCl

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭85￭ Remove the backup ring from the pump hea

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭86￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 3parts: a tip for removing the old piston seal a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭8712Figure 46 Removing the piston seal1Pisto

5.5 High pressure pump￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭88￭￭￭￭￭￭￭￭850 Professional IC Anion – MSM-HC – MCS – Prep 312Figure 48 Inserting the piston seal into the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation and maintenance850 Professional IC Anion – MSM-HC – MCS – Prep 3￭￭￭￭￭￭￭￭891234Figure 49 Removing valves1Outlet valve