Metrohm 855 Robotic Titrosampler Bedienungsanleitung

855 Robotic TitrosamplerManual8.855.8001EN

1.2 Instrument description￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭855 Robotic TitrosamplerControl. With the tiamo software the system can arbitrarily be extend

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction855 Robotic Titrosampler￭￭￭￭￭￭￭￭31.2.1 Model versionsThe 855 Robotic Titrosampler is available in the following

1.3 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭855 Robotic Titrosampler￭ Controller connectionFor connecting a PC or Touch Control.￭ Two US

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction855 Robotic Titrosampler￭￭￭￭￭￭￭￭5WarningThis symbol draws attention to a possible hazard dueto electrical current.

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭855 Robotic TitrosamplerWarningNever open the housing of the instrument. The instrument could be

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction855 Robotic Titrosampler￭￭￭￭￭￭￭￭71.4.4 Personnel safetyWarningWear protective goggles and working clothes suitabl

1.4 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭855 Robotic Titrosampler1.4.5 Flammable solvents and chemicalsWarningAll relevant safety measur

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument855 Robotic Titrosampler￭￭￭￭￭￭￭￭92 Overview of the instrument2.1 Front and rear123456789Figure 2 F

2.1 Front and rear￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭855 Robotic TitrosamplerUSB 2123456789Figure 3 Rear 855 Robotic Titrosampler1DistributorFor rinsing

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument855 Robotic Titrosampler￭￭￭￭￭￭￭￭112.2 Rear panelUSB 2USB 1Contr.MSB 1MSB 2MSB 3Made by MetrohmHeris

2.4 Sample racks￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭855 Robotic Titrosampler1Electrode connector (Ref.)For connecting reference electrodes. SocketB, 4 mm.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭133 Installation3.1 Setting up the instrument3.1.1 PackagingThe instrument is s

3.3 Connecting a computer￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭855 Robotic Titrosampler3.3 Connecting a computer The 855 Robotic Titrosampler requires a U

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭15For Windows Vista: The instrument is recognized and the installationassistant fo

3.5 Configuring the robotic arm￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭855 Robotic TitrosamplerIf the Swing Head is not connected, connect it as follows: 1Plu

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭17NoteA detailed list of the available robotic arms, along with the necessaryconfi

3.6 Mounting the robotic arm￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭855 Robotic Titrosampler5Max. swing angleThis stands for the swing range that therobotic a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭19Mounting the robotic armThe mounting of a robotic arm on the Swing Head is descr

3.7 Robotic arms with beaker sensor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭855 Robotic Titrosampler 3Screw the robotic arm to the Swing Head tightly with the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭21Functioning of the beaker sensorIf the beaker sensor of the robotic arm is activ

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] Robotic TitrosamplerManual8.855.8001E

3.8 Installing rinsing and aspiration equipment￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭855 Robotic Titrosampler6.1805.5106.1805.0606.1808.1706.1812.0001234Fig

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭23NoteThe opening of the tubing may need to be widened with a sharpobject (e.g. wi

3.9 Guide chain for cables and tubing￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭855 Robotic Titrosampler 3Fix the rinsing tubings￭ Place the rinsing tubings into

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭25CautionTake care to ensure when mounting tubing and cables that there is notract

3.10 Equipping the titration head￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭855 Robotic Titrosampler 2Insert the aspiration tip￭ Insert the 6.1543.170 aspiration

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭27 2Mount the stirring propeller￭ Fasten the 6.1909.050 stirring propeller to the

3.12 Connecting external pumps￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭855 Robotic TitrosamplerNoteIf an MSB stirrer is connected to the MSB1 socket, then the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭293.13 Connecting MSB devicesIn order to connect MSB devices, e.g.stirrers or dos

3.13 Connecting MSB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭855 Robotic Titrosampler3.13.1 Connecting dosing devicesThree dosing devices can be conne

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭313.13.2 Connecting a stirrer or titration standYou can use a magnetic stirrer 80

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

3.13 Connecting MSB devices￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭855 Robotic TitrosamplerNoteIf an MSB stirrer ist connected to the MSB1socket, then the st

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭333.14 Connecting USB devicesTwo USB connectors (Type A sockets) are available fo

3.15 Mounting the base plate￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭855 Robotic TitrosamplerSwitch the barcode reader to programming mode and make the followi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭35Proceed as follows: 1Insert the enclosed countersunk screw from below into the o

3.17 Attaching the sample rack￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭855 Robotic TitrosamplerInstall the drip pan as follows: 1Fasten the tubing enclosed to

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation855 Robotic Titrosampler￭￭￭￭￭￭￭￭37The rack is moved into starting position. The magnet code of the rackis read by

3.18 Mounting the safety shield￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭855 Robotic TitrosamplerNoteYou can adjust the vertical position of the safety shield a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Handling and maintenance855 Robotic Titrosampler￭￭￭￭￭￭￭￭394 Handling and maintenance4.1 GeneralThe 855 Robotic Titrosampler

5.1 Sample Processor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭855 Robotic Titrosampler5 Troubleshooting5.1 Sample ProcessorProblem Cause RemedyThe instrument

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Troubleshooting855 Robotic Titrosampler￭￭￭￭￭￭￭￭41Problem Cause RemedySwing Head – The SwingHead drive is defective.Contact the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents855 Robotic Titrosampler￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 The 855 Robotic Titrosampler in the

6.1 Beaker sensor￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭855 Robotic Titrosampler6 Appendix6.1 Beaker sensorEvery tower of a Sample Processor is equipped wi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Appendix855 Robotic Titrosampler￭￭￭￭￭￭￭￭43Figure 33 Spray nozzles - FunctioningThe height of the nozzles can be adjusted in th

6.3 Remote interface￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭855 Robotic Titrosampler6.3.1 Pin assignment of the remote interface13114251131425Figure 35 Pin a

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Appendix855 Robotic Titrosampler￭￭￭￭￭￭￭￭45Assigment Pin No. Assigment Pin No.Input 7 12 Output 7 20 volts / GND 14 Output 8 6+

6.5 Robotic arms￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭46￭￭￭￭￭￭￭￭855 Robotic Titrosampler6.5 Robotic arms6.5.1 Robotic arms for titrationTable 2 Configuration data o

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Appendix855 Robotic Titrosampler￭￭￭￭￭￭￭￭476.1462.260Robotic arm with holder for a titration head, left-swinging, exter-nalThe

6.5 Robotic arms￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭48￭￭￭￭￭￭￭￭855 Robotic Titrosampler6.1462.170Robotic arm with holder for a titration head and beaker sensor,right

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Appendix855 Robotic Titrosampler￭￭￭￭￭￭￭￭49Material: PP6.5.3 Robotic arms for special applicationsTable 5 Configuration data o

7.1 Measuring interface￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭50￭￭￭￭￭￭￭￭855 Robotic Titrosampler7 Technical specifications7.1 Measuring interfaceThe 855 Robotic Titr

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications855 Robotic Titrosampler￭￭￭￭￭￭￭￭51–1250…–1210 mV / +1210…+1250 mV: non-guaranteed values,dependent on

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭855 Robotic Titrosampler3.10 Equipping the titration head ...

7.3 Membrane pump(s) with valve￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭52￭￭￭￭￭￭￭￭855 Robotic Titrosampler7.3 Membrane pump(s) with valveDelivery rate> 450 mL/minPre

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Technical specifications855 Robotic Titrosampler￭￭￭￭￭￭￭￭537.6 Mains connectionVoltage100…240 VFrequency50…60 HzPower consump-

7.9 Ambient temperature￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭54￭￭￭￭￭￭￭￭855 Robotic Titrosampler7.9 Ambient temperatureNominal functionrange5…45 °CHumidity ＜ 80 %Sto

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty855 Robotic Titrosampler￭￭￭￭￭￭￭￭558 Conformity and warranty8.1 Declaration of ConformityThis is to ce

8.2 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭56￭￭￭￭￭￭￭￭855 Robotic TitrosamplerEN 61010-2-081 Particular requirements for automatic and semi

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Conformity and warranty855 Robotic Titrosampler￭￭￭￭￭￭￭￭57ComponentsAll components used in the Metrohm instruments have to sati

9.1 Scope of delivery 2.855.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭58￭￭￭￭￭￭￭￭855 Robotic Titrosampler9 AccessoriesNoteSubject to change without notice.9.1 Scope

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭59Qty. Order no. Description3 6.1805.060 FEP tubing / M6 / 60 cmWith light and kink

9.1 Scope of delivery 2.855.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭60￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description1 6.2053.000 Cable clipCable clip fo

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭61Qty. Order no. Description1 6.2621.030 Hexagon key 4 mmLength (mm): 731 6.2621.07

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents855 Robotic Titrosampler￭￭￭￭￭￭￭￭V7.2 Lift and turntable ...

9.1 Scope of delivery 2.855.0010￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭62￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description3 6.2740.020 Spray nozzleFor the fin

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭639.2 Scope of delivery 2.855.0020 Qty. Order no. Description1 1.855.0020 855 Robo

9.2 Scope of delivery 2.855.0020￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭64￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description3 6.1805.060 FEP tubing / M6 / 60 cm

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭65Qty. Order no. Description2 6.1812.000 PTFE tubing 4/6 mm, 4mMaterial: PTFEOuter

9.2 Scope of delivery 2.855.0020￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭66￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description1 6.2103.140 Adapter black 2 mm plug

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭67Qty. Order no. Description1 6.2621.130 Hexagon key 2 mm2 mm.1 6.2621.140 Hexagon

9.3 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭68￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description4 T.240.0102 Ferrite coresAnti-interference

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭69Qty. Order no. Description1 2.849.0010 849 Level ControlAdditional equipment for

9.3 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭70￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description1 6.1462.090 Robotic arm with Luer-Lock adap

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭71Qty. Order no. Description1 6.1462.170 Robotic arm with holder for titration head

Table of figures￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭VI￭￭￭￭￭￭￭￭855 Robotic TitrosamplerTable of figuresFigure 1 The Titrando system ...

9.3 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭72￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description1 6.1909.040 Stirring propeller / 102 mmProp

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭73Qty. Order no. Description1 6.2041.430 Sample rack 127 x 11 mLSample rack for 127

9.3 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭74￭￭￭￭￭￭￭￭855 Robotic TitrosamplerQty. Order no. Description1 6.2041.820 Sample rack 28 x 250 mLSample r

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Accessories855 Robotic Titrosampler￭￭￭￭￭￭￭￭75Qty. Order no. Description1 6.2141.300 Remote cable 843 Pump Station to SamplePro

Index￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭76￭￭￭￭￭￭￭￭855 Robotic TitrosamplerIndexNumbers/Symbols685 Dosimat ... 30700 Dosino ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index855 Robotic Titrosampler￭￭￭￭￭￭￭￭77Swing axis ... 17Swing direction ... 18

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction855 Robotic Titrosampler￭￭￭￭￭￭￭￭11 Introduction1.1 The 855 Robotic Titrosampler in the Titrando systemThe 855 R