Metrohm 800 Dosino Bedienungsanleitung

800 DosinoManual8.800.8002EN

1.2 About the documentation￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2￭￭￭￭￭￭￭￭800 Dosino1.2.1 Symbols and conventionsThe following symbols and styles are used in this do

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction800 Dosino￭￭￭￭￭￭￭￭31.3 Safety instructions1.3.1 General notes on safetyWarningThis instrument may only be operat

1.3 Safety instructions￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4￭￭￭￭￭￭￭￭800 DosinoProtection against electrostatic chargesWarningElectronic components are sensitive to

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭2 Overview of the instrument800 Dosino￭￭￭￭￭￭￭￭52 Overview of the instrument41235467910811Figure 1 800 Dosino1On LEDLights up, w

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6￭￭￭￭￭￭￭￭800 Dosino9Piston rodWith coupling. For moving the dosing pistonin the dosing unit.10Drive pinFor the rotation of the s

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation800 Dosino￭￭￭￭￭￭￭￭73 Installation3.1 Setting up the instrument3.1.1 PackagingThe instrument is supplied in high

3.2 Setting up the Dosino and the dosing unit￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8￭￭￭￭￭￭￭￭800 DosinoFigure 2 800 Dosino on the Titrando3.2.2 Dosino with bottle hol

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation800 Dosino￭￭￭￭￭￭￭￭93.2.3 Dosino on the canisterA Dosino with dosing unit can be mounted directly on a canister wh

3.2 Setting up the Dosino and the dosing unit￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10￭￭￭￭￭￭￭￭800 Dosino 2Set the holder for dosing units 6.2047.010 on the support rod

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation800 Dosino￭￭￭￭￭￭￭￭11All four dosing unit ports can be used with the free-standing supportassembly.3.2.5 Dosino wi

3.2 Setting up the Dosino and the dosing unit￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭12￭￭￭￭￭￭￭￭800 DosinoMounting the Dosino with the dosing unit6.1618.020Mount the Dos

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭3 Installation800 Dosino￭￭￭￭￭￭￭￭133.3 Connecting the 800 DosinoWarningConnect the Dosino only to control devices which have bee

3.3 Connecting the 800 Dosino￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭14￭￭￭￭￭￭￭￭800 Dosino 2Connect the connection cable of the Dosino to one of the socketsmarked with M

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Functioning800 Dosino￭￭￭￭￭￭￭￭154 FunctioningThe 800 Dosino forms, together with an 807 Dosing Unit (with 2, 5, 10,20 or 50 mL

4.1 Dosing/filling the dosing cylinder￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭16￭￭￭￭￭￭￭￭800 Dosino4.1 Dosing/filling the dosing cylinder1234567Figure 10 Dosing / Filli

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Functioning800 Dosino￭￭￭￭￭￭￭￭175Distributor discThe four holes in the distributor disc eachsets up a connection with one of th

4.2 Switching the stopcock￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭18￭￭￭￭￭￭￭￭800 Dosino4.2 Switching the stopcock123456Figure 11 Switching the stopcock1Drive pinfor the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭4 Functioning800 Dosino￭￭￭￭￭￭￭￭19The dosing drive sitting on the dosing unit turns, with the rotating drivepin, the centering tu

4.4 Standard assignment of the Dosino ports￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭20￭￭￭￭￭￭￭￭800 Dosino4.4 Standard assignment of the Dosino portsPort 1 Dosing outlet.

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation800 Dosino￭￭￭￭￭￭￭￭215 OperationIn this chapter you will learn the following regarding the handling of the800 Dosino

Metrohm AGCH-9101 HerisauSwitzerlandPhone +41 71 353 85 85Fax +41 71 353 89 [email protected] DosinoManual8.800.8002EN 09.2011 dm

5.1 Attaching the Dosino onto the dosing unit￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭22￭￭￭￭￭￭￭￭800 Dosino 2Check the position of the centering tube of the dosing unit12

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation800 Dosino￭￭￭￭￭￭￭￭231234Figure 16 Mounting the 800 Dosino onto the 807 Dosing Unit1Green line marking2Guide pins3UNLO

5.2 Problems when attaching the Dosino￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭24￭￭￭￭￭￭￭￭800 Dosino5.2 Problems when attaching the DosinoIf the 800 Dosino cannot be att

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation800 Dosino￭￭￭￭￭￭￭￭25 6Turn the dosing unit upside-down and press it together against atabletop.The piston stopper sho

5.4 Reagent exchange￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭26￭￭￭￭￭￭￭￭800 Dosino 2Check whether the Status LED of the dosing drive is lit up. 3Rotate the Dosino to the

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭5 Operation800 Dosino￭￭￭￭￭￭￭￭27NoteIf you do not use a reagent for more than one week, empty the dosingunit with the EMPTY/Empty

5.5 Function of the LEDs￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭28￭￭￭￭￭￭￭￭800 DosinoThe LED flashes fastThe 800 Dosino has detected a malfunction. This could involve, f

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance800 Dosino￭￭￭￭￭￭￭￭296 Handling and maintenance6.1 General information6.1.1 CareIn contrast to the d

6.2 Quality Management and validation with Metrohm￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭30￭￭￭￭￭￭￭￭800 Dosino6.1.2 Maintenance by Metrohm ServiceMaintenance of the 80

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭6 Handling and maintenance800 Dosino￭￭￭￭￭￭￭￭316.3 GLP - ValidationEvery drive and every dosing unit manufactured by the Metrohm

TeachwareMetrohm AGCH-9101 [email protected] documentation is protected by copyright. All rights reserved.Although all the information

7.1 Problems￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭32￭￭￭￭￭￭￭￭800 Dosino7 Troubleshooting7.1 ProblemsProblem Cause RemedyData of the dosingunit cannot be read.Data ch

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭7 Troubleshooting800 Dosino￭￭￭￭￭￭￭￭33Problem Cause RemedyThe Dosino cannotbe attached to thedosing unit.Thedrive pin of the dosi

7.1 Problems￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭34￭￭￭￭￭￭￭￭800 DosinoProblem Cause Remedy4. Place the dosing unit with Dosino attachedupright on the distributor, ali

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭8 Appendix800 Dosino￭￭￭￭￭￭￭￭358 Appendix8.1 Buret dataThe 807 Dosing Units are equipped with a data chip which contains thespe

8.1 Buret data￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭36￭￭￭￭￭￭￭￭800 Dosino21Figure 19 Data chip and contact pin1Contact surfaceon the 800 Dosino2Data chip with contact

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭9 Technical specifications800 Dosino￭￭￭￭￭￭￭￭379 Technical specifications9.1 Dosing driveResolution10000 steps per cylinder vol

9.4 Electromagnetic compatibility (EMC)￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭38￭￭￭￭￭￭￭￭800 Dosino9.4 Electromagnetic compatibility (EMC)EmissionStandards fulfilled:￭

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10 Conformity and warranty800 Dosino￭￭￭￭￭￭￭￭3910 Conformity and warranty10.1 Declaration of ConformityThis is to certify the co

10.2 Quality Management Principles￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭40￭￭￭￭￭￭￭￭800 DosinoMetrohm Ltd. is holder of the SQS certificate ISO 9001:2000 Quality man-ag

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭10 Conformity and warranty800 Dosino￭￭￭￭￭￭￭￭41ManufactureThe measures put into practice in the production of our instruments gua

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of contents800 Dosino￭￭￭￭￭￭￭￭IIITable of contents1 Introduction 11.1 Instrument description ...

11.1 Scope of delivery￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭42￭￭￭￭￭￭￭￭800 Dosino11 Accessories11.1 Scope of deliveryNoteSubject to change without notice.11.1.1 800

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭11 Accessories800 Dosino￭￭￭￭￭￭￭￭43Qty. Order no. Description1 6.1546.030 Piston tongsFor the PTFE pistons of the dosing unit1 8.

11.2 Optional accessories￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭44￭￭￭￭￭￭￭￭800 DosinoOrder no. Description6.3032.150 Dosing unit 5 mLDosing unit with integrated data ch

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Index800 Dosino￭￭￭￭￭￭￭￭45IndexAAccuracy ... 31Adsorber tube ... 20Air inle

Table of contents￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭IV￭￭￭￭￭￭￭￭800 Dosino6 Handling and maintenance 296.1 General information ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭Table of figures800 Dosino￭￭￭￭￭￭￭￭VTable of figuresFigure 1 800 Dosino ...

￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭￭1 Introduction800 Dosino￭￭￭￭￭￭￭￭11 IntroductionThe 800 Dosino is a versatile dosing drive which can be used with a num-ber of d